HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 594380, compound → HCID 2834903, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 594380 | HCID 594380 | — |
| Reactant | HCID 20312263 | HCID 20312263 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 2834903 | HCID 2834903 | — |
Reaction Steps
Phenanthridinium perchlorate (2 g) and 4-phenylpent-3-ene-2-one (4 g) were heated together at 150° for 16 hours. The reaction mixture was cooled and diluted with methanol. The product was isolated by filtration and recrystallized from acetonitrile. Yield 1.5 g, m.p. 252°-3°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04108667 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-9e579a6f58994ed590822f029d6032e2 |
| Source note | uspto-grants-1978_08 |