HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12220937, compound → HCID 12220950, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12220937 | HCID 12220937 | — |
| Reactant | HCID 20312280 | HCID 20312280 | — |
| Product | HCID 12220950 | HCID 12220950 | — |
Reaction Steps
3,4-Dihydroisoquinolinium perchlorate (1.2 g) and 2-isopropylidenebenzothien-3-one-1,1-dioxide (2 g) were heated together at 150° for 16 hours. The reaction mixture was triturated with hot methanol and filtered. The product was purified by recrystallization from acetonitrile. Yield 0.6 g, m.p. > 330°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04108667 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-cd9ffa57652b4da2a945d67a14fc0966 |
| Source note | uspto-grants-1978_08 |