Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Styrene Oxide | HCID 7276 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 4-Mercaptophenol | HCID 240147 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20312354 | HCID 20312354 | — |
Reaction Steps
4-Mercaptophenol (63 grams) and 0.5 gram of KOH were combined in a flask equipped with an agitator, water condenser and thermometer. The combination was heated to 120° C. under nitrogen. Styrene oxide (66 grams) was added dropwise at 100° C. to 135° C. The combination was neutralized with one millimeter of hydrochloric acid and the volatiles stripped off to a pot temperature of 170° C. at 28 millimeters of mercury. The weight of product was 131 grams.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04108831 |
|---|
| Source dataset | uspto-grants-1978_08 |
|---|
| ORD ID | ord-3fa69f48f264450fac2136c473d72d95 |
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| Source note | uspto-grants-1978_08 |
|---|
