Hydrochloric Acid → HCID 20312354, compound

HRID 2419988Notes

Reaction equation

HRID 2419988 reaction equation
[SH:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][CH:3]=1.[OH-].[K+].[CH2:11]1[O:19][CH:12]1[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1.Cl>O>[OH:19][CH:12]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[CH2:11][S:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][CH:3]=1

Participants

6

Reactant 4

HCID 313Hydrochloric AcidHCID 7276Styrene OxideHCID 14797Potassium HydroxideHCID 2401474-Mercaptophenol

Product 1

HCID 20312354HCID 20312354, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
120 °C

Procedure

4-Mercaptophenol (63 grams) and 0.5 gram of KOH were combined in a flask equipped with an agitator, water condenser and thermometer. The combination was heated to 120° C. under nitrogen. Styrene oxide (66 grams) was added dropwise at 100° C. to 135° C. The combination was neutralized with one millimeter of hydrochloric acid and the volatiles stripped off to a pot temperature of 170° C. at 28 millimeters of mercury. The weight of product was 131 grams.

Workup

  1. customstripped off to a pot temperature of 170° C. at 28 millimeters of mercury

Sources & evidence

ORD record
ord-3fa69f48f264450fac2136c473d72d95
Source dataset
uspto-grants-1978_08
Patent number
US04108831

Reaction notes

Loading…