HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroethanol → 4-((2-Hydroxyethyl)thio)phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroethanol | HCID 34 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 4-Mercaptophenol | HCID 240147 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-((2-Hydroxyethyl)thio)phenol | HCID 13052632 | — |
Reaction Steps
4-Mercaptophenol (126 grams) was dissolved in 60 millimeters of ethanol. A solution of KOH (58 grams) dissolved in ethanol (150 millimeters) was added under a nitrogen blanket. 2-Chloroethanol (83 grams) was then added slowly and the combination allowed to react for 11/2 hours. The product was filtered and the volatiles stripped off. The weight of product was 172 grams.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04108831 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-d6dbcffb7d864790b4458d067bbffacf |
| Source note | uspto-grants-1978_08 |