HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Propanediamine → HCID 20312555, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Propanediamine | HCID 428 | — |
| Reactant | Pentachloropyridine | HCID 16584 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 20312555 | HCID 20312555 | 57% |
Reaction Steps
Using the same procedure as in Example 2, 25.1 g. (0.1 mole) of pentachloropyridine in 200 ml. of THF was caused to react with 22.3 g. (0.3 mole) of 1,3-propanediamine in 200 ml. of THF to give 18.6 g. (57%) of the title compound, melting at 248°-9°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04108859 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-47461cdcb7794b84830055c6bb068e5d |
| Source note | uspto-grants-1978_08 |