1,3-Propanediamine → HCID 20312555, compound

HRID 2420000Notes

Reaction equation

HRID 2420000 reaction equation
[Cl:1][C:2]1[N:7]=[C:6]([Cl:8])[C:5]([Cl:9])=[C:4](Cl)[C:3]=1[Cl:11].[CH2:12]([NH2:16])[CH2:13][CH2:14][NH2:15]>C1COCC1>[ClH:1].[Cl:8][C:6]1[C:5]([Cl:9])=[C:4]([NH:15][CH2:14][CH2:13][CH2:12][NH2:16])[C:3]([Cl:11])=[C:2]([Cl:1])[N:7]=1

Participants

4

Reactant 2

HCID 4281,3-PropanediamineHCID 16584Pentachloropyridine

Product 1

HCID 20312555HCID 20312555, compoundYield 57%

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent2×

Procedure

Using the same procedure as in Example 2, 25.1 g. (0.1 mole) of pentachloropyridine in 200 ml. of THF was caused to react with 22.3 g. (0.3 mole) of 1,3-propanediamine in 200 ml. of THF to give 18.6 g. (57%) of the title compound, melting at 248°-9°.

Workup

  1. customto react with 22.3 g

Sources & evidence

ORD record
ord-47461cdcb7794b84830055c6bb068e5d
Source dataset
uspto-grants-1978_08
Patent number
US04108859

Reaction notes

Loading…