HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 54023871, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | tert-Butyl 2-bromopropanoate | HCID 545327 | — |
| Reactant | N-Hydroxy-L-alanine | HCID 18605011 | — |
| Product | HCID 54023871 | HCID 54023871 | — |
Reaction Steps
17.7 g. of the tert-butyl ester of N-hydroxyalanine which was prepared from tert-butyl bromopropionate by the method of Newman et al. [J. Amer. Chem. Soc. 77, 2308 (1971)] was added to 40 ml. of acetic anhydride and the mixture was stirred for 30° minutes at 100° C. The reaction mixture was evaporated to dryness under reduced pressure to give the oily tert-butyl ester of N-acetyl-N-acetoxyalanine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04108861 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-97bdfb943d9b409c949aa460957f2ae6 |
| Source note | uspto-grants-1978_08 |