HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → 1-Benzyl-3,4-diethylpyridin-1-ium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | 3,4-Diethylpyridine | HCID 69151 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | 1-Benzyl-3,4-diethylpyridin-1-ium chloride | HCID 20338110 | — |
Reaction Steps
Benzyl chloride (250 g.) was added dropwise to a stirred and refluxed solution of 3,4-diethylpyridine (262 g.) and isopropyl alcohol (700 ml.). Repeated concentration under vacuum and addition of benzene afforded a slurry of crystalline 1-benzyl-3,4-diethyl-pyridinium chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04108857 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-84e712d38cec4785bd027dd88436149f |
| Source note | uspto-grants-1978_08 |