HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 53886440, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 20313024 | HCID 20313024 | — |
| Product | HCID 53886440 | HCID 53886440 | — |
Reaction Steps
To one gram of ethyl 5-benzylpicolinate, 10 ml. of 28% aqueous ammonia were added. After allowing the mixture to stand at room temperature for 24 hours, crystals formed were collected by filtration and recrystallized from ethanol to obtain 0.6 g of 5-benzylpicolinic acid amide as colorless crystals of a melting point of 193°~196° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04109000 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-9d7561ad9af4449ba94e0238ef3a01f1 |
| Source note | uspto-grants-1978_08 |