HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20313223, compound → HCID 20313231, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20313223 | HCID 20313223 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 20313231 | HCID 20313231 | — |
Reaction Steps
In 250 ml. of anhydrous tetrahydrofuran was suspended 2.0 g. of lithium aluminum hydride and then a solution prepared by dissolving 8.0 g. of 4-butyl-2-(7-indenyloxymethyl)morpholin-5-one in 50 ml. of anhydrous tetrahydrofuran was added slowly to the suspension with stirring. Then, by treating the mixture in a similar manner as in Example 1, 6.4 g. (yield) of oily 4-butyl-2-(7-indenyloxymethyl)-morpholine was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04109088 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-a067caeea1674e1798d17031c2f92526 |
| Source note | uspto-grants-1978_08 |