HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20313213, compound → HCID 20313218, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20313213 | HCID 20313213 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 20313218 | HCID 20313218 | 38% |
Reaction Steps
In 200 ml. of anhydrous tetrahydrofuran was suspended 1.4 g. of lithium aluminum hydride and after adding thereto slowly a solution prepared by dissolving 5.8 g. of 2-(7-indenyloxymethyl)-4-methylmorpholin-5-one in 30 ml. of tetrahydrofuran, the mixture was treated in a similar manner as in Example 1 to provide 2.1 g. (yield 38%) of oily 2-(7-indenyloxymethyl)-4-methylmorpholine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04109088 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-a509a62614434aa58730184fd5dc1959 |
| Source note | uspto-grants-1978_08 |