HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12917368, compound → HCID 12917376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12917368 | HCID 12917368 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 12917376 | HCID 12917376 | 89% |
Reaction Steps
In 300 ml. of anhydrous tetrahydrofuran was suspended 20 g. of lithium aluminum hydride and after adding slowly to the suspension a solution prepared by dissolving 8.0 g. of 4-benzyl-2-(7-indenyloxymethyl)morpholin-5-one in 50 ml. of tetrahydrofuran, the mixture was treated in a similar manner as in Example 1 to provide 6.8 g. (yield 89%) of oily 4-benzyl-2-(7-indenyloxymethyl)morpholine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04109088 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-2a2e1a00680c48818b49a9b754ac103e |
| Source note | uspto-grants-1978_08 |