HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20313216, compound → HCID 20313226, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20313216 | HCID 20313216 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 20313226 | HCID 20313226 | 89.5% |
Reaction Steps
In 50 ml. of anhydrous tetrahydrofuran was suspended 0.5 g. of lithium aluminum hydride and after adding slowly to the suspension a solution prepared by dissolving 2.0 g. of 2-(7-indenyloxymethyl)-4-propylmorpholin-5-one in 10 ml. of anhydrous tetrahydrofuran, the mixture was treated in a similar manner as in Example 1 to provide 1.7 g. (yield 89.5%) of oily 2-(7-indenyloxymethyl)-4-propylmorpholine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04109088 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-9cc6b6151f654d9ab4d4c4616c70191d |
| Source note | uspto-grants-1978_08 |