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HRID2420183

反应详情

EQUATION

反应方程式

HRID 2420183 的结构方程式

REACTANTS

反应物

2
结构：O=P(O)(O)O
HCID1004

Phosphoric acid

H3O4P

结构：[Na+].[Na+].[O]=[W](=[O])([O-])[O-]
HCID26052

未命名化合物

PRODUCTS

生成物

1
结构：O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.P.[W].[W].[W].[W].[W].[W].[W].[W].[W].[W].[W].[W]
HCID452313

Phosphane--tungsten--water (1/12/40)

H83O40PW12

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

Phosphotungstic acid reagent was prepared by refluxing a solution of 4 g sodium tungstate in 30 ml of H2O with 3.2 ml of 85% by weight orthophosphoric acid for 2 hours. The solution was then cooled to room temperature and diluted to 100 cc. Then 3.2 g of Li2SO4.H2O was added and mixed well. This liquid reagent material was incorporated into pods prepared as described in Example 1.

WORKUP

后处理

  1. additiondiluted to 100 cc
  2. additionmixed well
  3. customprepared