HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20311078, compound → HCID 20311079, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20311078 | HCID 20311078 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20311079 | HCID 20311079 | 74.4% |
Reaction Steps
The product of Stage 5 (4.0 g) is dissolved with heating in 250 ml of ethanol and catalytically hydrogenated with Raney nickel at 50° C./50 atms pressure. Concentration of the hydrogenation solution after the nickel has been filtered off under suction gives 2.8 g of a product melting at 75°-76° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04110113 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-aaae87a00ec9468ebdad887762179cd2 |
| Source note | uspto-grants-1978_08 |