HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl p-methylbenzenesulfonate → HCID 20311111, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl p-methylbenzenesulfonate | HCID 6638 | — |
| Reactant | 5,7-Dichloro-2,6-dimethylbenzoxazole | HCID 14419019 | — |
| Product | HCID 20311111 | HCID 20311111 | — |
Reaction Steps
A mixture of 2.1 g. of 2,6-dimethyl-5,7dichloro-benzoxazole and 2 g. of ethyl-p-toluene-sulfonate was heated at 150° C. for 30 minutes. By cooling, a pick cake was obtained. It was ground in a mortar by washing repeatedly with ethyl ether. The product, thus obtained, was dried and used without further purification for the synthesis of dyes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04110116 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-9d9400fc9b4b4a259ff7ef6a37afdcf6 |
| Source note | uspto-grants-1978_08 |