HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20311331, compound → HCID 20311328, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20311331 | HCID 20311331 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 20311328 | HCID 20311328 | — |
Reaction Steps
32.6 g (mol/7.8) of 2-methyl-(2'-nitro-4'-methoxyanilino)-propionic acid, in solution in 330 ml of tetrahydrofuran, are hydrogenated in the presence of 20 g of Raney nickel in an autoclave with a capacity of 500 ml. Hydrogen pressure in the cold: 150 kg/cm2. Temperature = 70°-90° C.; Duration: 3 hours
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04110337 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-e955d19f2e6e4404983f7dcfc27f158a |
| Source note | uspto-grants-1978_08 |