HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorobenzylamine → HCID 56847143, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorobenzylamine | HCID 66853 | — |
| Reactant | HCID 86662688 | HCID 86662688 | — |
| Product | HCID 56847143 | HCID 56847143 | 42% |
Reaction Steps
Reaction of 220 mg (0.73 mmol) 1,4-dimethyl-2-thioxo-7-(trifluoromethyl)-1H-quinoline-3-carboxylic acid with 3-fluoro-benzylamine according to the method described under example 2 Section a) yielded 125 mg (0.3 mmol, 42%) N-[(3-fluorophenyl)-methyl]-1,4-dimethyl-2-thioxo-7-(trifluoromethyl)-1H-quinoline-3-carboxylic acid amide (example 3). MS: m/z 409.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08653102B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-4dcba4f1a04b4e36b3677852b3555942 |
| Source note | uspto-grants-2014_02 |