Sodium Hydroxide → HCID 20311664, compound

Participants

Reaction Steps

The starting material is prepared as follows: The mixture of 4.6 g of dl-1-(4-benzyloxyphenyl)-2-(2,2-diphenylethylamino)-propane hydrochloride, 0.4 g of sodium hydroxide, 50 ml of ethanol and 0.5 g of 10% palladium on carbon is shaken under hydrogen at 3 atmospheres for 72 hours. The mixture is filtered and the filtrate evaporated, to afford the 1-(4-hydroxyphenyl)-2-(2,2-diphenylethylamino)-propane, which is used without further purification.

Provenance & Evidence