Hydrogen iodide → HCID 70596994, compound

HRID 2420611Notes

Reaction equation

HRID 2420611 reaction equation
[O:1]1[CH2:6][CH2:5][N:4]([CH2:7][CH2:8][C:9]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=2[C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)(O)[CH3:10])[CH2:3][CH2:2]1.I>C(O)(=O)C>[O:1]1[CH2:6][CH2:5][N:4]([CH2:7][CH2:8][CH:9]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=2[C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[CH3:10])[CH2:3][CH2:2]1

Participants

4

Reactant 2

HCID 24841Hydrogen iodideHCID 70595222HCID 70595222, compound

Product 1

HCID 70596994HCID 70596994, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

A mixture of 3.1 g of 1-morpholino-3-p-biphenylyl-butan-3-ol, 10 ml of 67% hydriodic acid and 18 ml of acetic acid is heated at 150° for 1.5 hours. 1-Morpholino-3-p-biphenylyl-butane is obtained after cooling and working up in the customary manner.

Workup

  1. temperatureis heated at 150° for 1.5 hours

Sources & evidence

ORD record
ord-350922eed5844373a8c1ab7bd5f0f7f5
Source dataset
uspto-grants-1978_08
Patent number
US04110447

Reaction notes

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