Hydrochloric Acid → HCID 67215364, compound

Participants

Reaction Steps

[11-(1H-Imidazol-2-ylcarbarmoyl)undecyl]carbamic acid tert-butyl ester (13) (0.060 g, 0.16 mmol) was treated with 4 M HCl in dioxane (2 mL, 8 mmol) and the mixture stirred at room temperature for 14 hours. The reaction mixture was concentrated in vacuo and further dried under high vacuum. The resulting white solid (0.056 g, 99%) was used directly without further purification. m/z (ESI) 281 [C15H28N4O+H]+.

Provenance & Evidence