HCID 178470516, compound → HCID 178524963, compound

Participants

Reaction Conditions

Reaction Steps

Ethyl 5-[(2,2,2-trifluoroethyl)thio]-1H-1,2,3-triazole-4-carboxylate (0.086 g) was suspended in 1N aqueous sodium hydroxide solution and heated at 70° C. for 3 h. The reaction mixture was filtered and then acidified with concentrated hydrochloric acid. Concentration in vacuo afforded a colourless solid which was washed with ice cold water to afford the subtitle compound (0.080 g)

Provenance & Evidence