HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178524962, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 178470511 | HCID 178470511 | — |
| Product | HCID 178524962 | HCID 178524962 | 83.7% |
Reaction Steps
Ethyl 5-(trifluoromethyl)-1H-1,2,3-triazole-4-carboxylate (0.312 g) was stirred in aqueous N sodium hydroxide (3.8 mL) and heated under reflux for 90 min. The cooled solution was acidified with aqueous hydrochloric acid and extracted with ethyl acetate. The extracts were washed with brine then dried and evaporated to leave a colourless solid (0.226 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07956070B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-7c704846f6924702bc17e785b104b44d |
| Source note | uspto-grants-2011_06 |