Sodium Hydroxide → HCID 178482485, compound

Participants

Reaction Steps

Methyl 5-[methyl(methylsulfonyl)amino]-1H-1,2,3-triazole-4-carboxylate (0.36 g) was stirred in THF (5 mL) with 2 N aqueous sodium hydroxide solution (1.7 mL) for 18 h. The mixture was concentrated in vacuo. To the aqueous residue was added dilute acetic acid and this was extracted with ethyl acetate (2×15 mL). The extracts were washed with water and brine then dried and evaporated to leave the subtitle compound (0.07 g).

Provenance & Evidence