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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2421074Generated: October 31, 2026

Hydrochloric Acid → HCID 59025450, compound

https://huagongshe.com/reaction/2421074

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 59025429HCID 59025429—
SolventMethanolHCID 887—
ProductHCID 59025450HCID 59025450—

Reaction Steps

Tert-butyl 4-[(3aS,7aS)-3-allyl-2-oxooctahydro-1H-benzimidazol-1-yl]piperidine-1-carboxylate was dissolved in methanol (20 mL) and 4 M HCl (7 mL) was then added. The mixture was stirred at room temperature and then concentrated in vacuo. The salt was then converted to freebase by using MP-carbonate. MS (M+1): 264.2.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07956069B2
Source datasetuspto-grants-2011_06
ORD IDord-8350971c4e724581bb7bfb6b42a30eab
Source noteuspto-grants-2011_06