HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane hydrochloride → HCID 59025420, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 59025416 | HCID 59025416 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59025420 | HCID 59025420 | — |
Reaction Steps
tert-butyl 4-[(3aR,7aS)-2-oxooctahydro-1H-indol-1-yl]piperidine-1-carboxylate was dissolved in MeOH (25 mL) and 4M HCl/dioxane (5 mL) was added. The mixture stirred at room temperature then concentrated in vacuo to give the tile compound. MS (M+1): 223.26
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07956069B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-f87dbdfb2e2646619e81ee26ce0fb60f |
| Source note | uspto-grants-2011_06 |