HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 59025434, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 59025447 | HCID 59025447 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59025434 | HCID 59025434 | 89.3% |
Reaction Steps
To a solution of tert-butyl 4-[(3aR,7aS)-2-oxooctahydro-1H-indol-1-yl]-1,4′-bipiperidine-1′-carboxylate (180 mg, 0.44 mmol) in MeOH (3 mL) was added 4M HCl (1 mL) and the mixture was stirred at room temperature. The solvents were then removed under reduced pressure to provide the title compound as yellow oil (120 mg). Ms (M+1): 306.3
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07956069B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-cfd543b4b5ca478bad2970573288d5fa |
| Source note | uspto-grants-2011_06 |