HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 21914345, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Piperidine, 1-(2-chloroethyl)-, hydrochloride | HCID 74826 | — |
| Reactant | HCID 21914379 | HCID 21914379 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 21914345 | HCID 21914345 | 60.7% |
Reaction Steps
N-(4-Bromo-3-hydroxyphenyl)acetamide (19.4 g), anhydrous potassium carbonate (25.6 g), 1-(2 chloroethyl)piperidine hydrochloride (15.78 g) and acetone (400 ml) were heated at reflux for 18 h, filtered and evaporated to dryness to give the product as a solid (17.48 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07956084B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-09888266b3b7463b8465dde2fbec876d |
| Source note | uspto-grants-2011_06 |