HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → HCID 57762479, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | 2,6-Dimethylbenzoic acid | HCID 12439 | — |
| Product | HCID 57762479 | HCID 57762479 | — |
Reaction Steps
Using Preparation Method 1, 2,6-dimethylbenzoic acid was reacted with isopropylamine. The resulting reaction mixture was purified using SiO2 with CH2Cl2/MeOH 99:1. A white crystalline solid was obtained (73%). NMR 1H (ppm, CDCl3): 7.15-7.10 (m, 1H), 6.99 (d, J3=7.57 Hz, 2H), 5.44 (br. s., 1H), 4.40-4.24 (m, 1H), 2.31 (s, 6H), 1.24 (d, J3=6.58 Hz, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07956216B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-5058dd5d63024cb3a79c7bc7eb710a2a |
| Source note | uspto-grants-2011_06 |