HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxybenzoic Acid → Poly(4-hydroxybenzoic acid-co-6-hydroxy-2-naphthoic acid)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxybenzoic Acid | HCID 135 | — |
| Reactant | Oxo(oxostibanyloxy)stibane | HCID 27652 | — |
| Reactant | 6-Hydroxy-2-naphthoic acid | HCID 85557 | — |
| Product | Poly(4-hydroxybenzoic acid-co-6-hydroxy-2-naphthoic acid) | HCID 16212814 | — |
Reaction Steps
Charging was conducted at a ratio of 0.6 mol of parahydroxybenzoic acid (PHBA) per mol of 6-hydroxy-2-naphthoic acid (HNCA), 110 ppm of a catalyst in the form of antimony trioxide was added based on the number of mols of HNCA, and the mixture was reacted for 4 hours at 300° C. under reduced pressure. Strands of molten polymer were extruded from the outlet, cooled, and cut to obtain HNCA+PHBA pellets.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07960045B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-2ca7eb495a314852970b194175f3b74b |
| Source note | uspto-grants-2011_06 |