HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropylamine → HCID 67243228, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Reactant | HCID 67243508 | HCID 67243508 | — |
| Product | HCID 67243228 | HCID 67243228 | 59% |
Reaction Steps
2.07 g (4.6 mmoles) 8-chloro-4-methyl-1-(3-methyl-4-nitrophenyl)-3H-2,3-benzodiazepine-3-carboxylic acid phenyl ester are boiled in 10 ml of cyclopropylamine for 10 hours. The separated crystals are filtered off, and the crude product is re-crystallized from ethanol. Thus 1.12 g (59%) of the desired compound melting at 221-223° C. is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07960375B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-7e3eb58fe9534808afe9df46a8dc10ce |
| Source note | uspto-grants-2011_06 |