Hydrochloric Acid → HCID 67242897, compound

Participants

Reaction Steps

1.59 g of 2 (3.78 mmol) are placed in a 100 mL round-bottomed flask and 25 mL of a solution of hydrogen chloride in dioxane (4 M) are added. The medium is stirred for 5 hours at room temperature under argon. After evaporating off the solvent, 1.44 g of amine 3 are obtained in hydrochloride form, which product is used directly for the following step.

Provenance & Evidence