Hydrochloric Acid → HCID 67242544, compound

Participants

Reaction Steps

10 mL of a solution of hydrogen chloride in dioxane (4 M) are added to a 25 mL round-bottomed flask containing 500 mg of 20 (1.34 mmol). The mixture is stirred for 4 hours at room temperature under argon. A white precipitate forms, which is filtered off by suction and washed with 3 mL of dioxane and then 5 mL of isopropyl ether. 386 mg of amine 21 (beige-coloured solid) are thus obtained in the form of hydrochloride.

Provenance & Evidence