Hydrochloric Acid → HCID 67242480, compound

Participants

Reaction Steps

8 mL of a solution of hydrogen chloride in dioxane (4 M) are placed in a 50 mL round-bottomed flask containing 410 mg of 40 (1.107 mmol). The mixture is stirred for 4 hours at room temperature under argon. A white precipitate forms, which is filtered off by suction and washed with 3 mL of dioxane and then 5 mL of isopropyl ether. 260 mg of amine 41 (white solid) are thus obtained in the form of the hydrochloride.

Provenance & Evidence