Hydrochloric Acid → HCID 67241054, compound

Participants

Reaction Steps

2.6 mL of a solution of hydrogen chloride in dioxane (4 M) are added to a 25 mL round-bottomed flask containing 139 mg of 45 (0.352 mmol). The mixture is stirred for 4 hours at room temperature under argon. A white precipitate forms, which is filtered off by suction and washed with 3 mL of dioxane and then 5 mL of isopropyl ether. 72 mg of amine 46 (white solid) are thus obtained in the form of the hydrochloride.

Provenance & Evidence