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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2421867Generated: November 2, 2026

Hydrochloric Acid → HCID 67243260, compound

https://huagongshe.com/reaction/2421867

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 86629182HCID 86629182—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 67243260HCID 67243260—

Reaction Steps

1.6 mL of a solution of hydrogen chloride in dioxane (4 M) are added to a 25 mL round-bottomed flask containing 68.4 mg of 50 (0.219 mmol). The mixture is stirred for 4 hours at room temperature under argon. After concentrating the reaction medium to dryness, 51 mg of amine 51 (yellow solid) are thus obtained in the form of the hydrochloride.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07960373B2
Source datasetuspto-grants-2011_06
ORD IDord-5bfa3a66067343e0b192981d52e132c1
Source noteuspto-grants-2011_06