HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67243260, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86629182 | HCID 86629182 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 67243260 | HCID 67243260 | — |
Reaction Steps
1.6 mL of a solution of hydrogen chloride in dioxane (4 M) are added to a 25 mL round-bottomed flask containing 68.4 mg of 50 (0.219 mmol). The mixture is stirred for 4 hours at room temperature under argon. After concentrating the reaction medium to dryness, 51 mg of amine 51 (yellow solid) are thus obtained in the form of the hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07960373B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-5bfa3a66067343e0b192981d52e132c1 |
| Source note | uspto-grants-2011_06 |