Hydrochloric Acid → HCID 67240807, compound

Participants

Reaction Steps

10.4 mL of a solution of hydrogen chloride in dioxane (4 M) are placed in a 100 mL round-bottomed flask containing 450 mg of 55 (1.387 mmol). The mixture is stirred for 3 hours at room temperature under argon. A white precipitate forms, which is filtered off by suction and washed with 3 mL of dioxane and then 5 mL of isopropyl ether. 259 mg of amine 56 (cream-coloured solid) are thus obtained in the form of the hydrochloride.

Provenance & Evidence