Hydrochloric Acid → HCID 67242126, compound

Participants

Reaction Steps

3.65 mL of a solution of hydrogen chloride in dioxane (4 M) are placed in a 100 mL round-bottomed flask containing 188 mg of 60 (0.487 mmol). The reaction medium is concentrated to dryness and the residue is taken up in 10 mL of isopropyl ether. After filtering, 100 mg of amine 61 (white solid) are obtained in the form of the hydrochloride.

Provenance & Evidence