HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3-Chlorophenyl)piperazine → HCID 58834857, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3-Chlorophenyl)piperazine | HCID 1355 | — |
| Reactant | 4-Chloro-2-methylphenyl isocyanate | HCID 142157 | — |
| Reactant | HCID 11826263 | HCID 11826263 | — |
| Product | HCID 58834857 | HCID 58834857 | — |
Reaction Steps
Starting with 150 mg (0.34 mmol) of the iminophosphorane from Example 3A, 60 mg (0.36 mmol) of 4-chloro-2-methylphenyl isocyanate and 67 mg (0.34 mmol) of N-(3-chlorophenyl)piperazine, the general procedure [E] and chromatographic purification (method 2) give 97 mg (46% of theory) of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07960387B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-6eb7615f307846589e8ff86609869e32 |
| Source note | uspto-grants-2011_06 |