HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67242996, compound → HCID 178462963, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67242996 | HCID 67242996 | — |
| Reactant | HCID 178419017 | HCID 178419017 | — |
| Product | HCID 178462963 | HCID 178462963 | — |
Reaction Steps
The title compound was prepared from 4-chloro-2-ethyl-5-phenylisothiazol-3(2H)-one 1,1-dioxide and 2-(1H-imidazol-4-yl)ethanamine in a similar manner as described for Example 1. 1H NMR (500 MHz, CD3OD): δ 7.54-7.42 (m, 6H), 6.51-6.48 (m, 1H), 3.71 (q, 2H), 3.14 (t, 2H), 2.55 (t, 2H), 1.36 (t, 3H); 13C NMR (125 MHz, CD3OD): δ 159.9, 137.3, 136.1, 132.9, 132.3, 130.6, 129.7, 126.9, 117.2, 107.2, 44.6, 36.0, 27.8, 14.0; Mass Spectrum: M+H+ 347.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07960380B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-116bfe68031d44baade59fbd4e955a0d |
| Source note | uspto-grants-2011_06 |