Methylamine → HCID 11632547, compound
Reaction equation
[NH2:1][C:2]1[CH:10]=[C:9]([CH3:11])[CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=O.[CH3:12][NH2:13].[N:14]1([CH2:20][CH2:21][CH2:22][O:23][C:24]2[CH:31]=[CH:30][C:27]([CH:28]=O)=[CH:26][CH:25]=2)[CH2:19][CH2:18][CH2:17][CH2:16][CH2:15]1>>[CH3:12][N:13]1[C:4](=[O:6])[C:3]2[C:2](=[CH:10][C:9]([CH3:11])=[CH:8][CH:7]=2)[N:1]=[C:28]1[C:27]1[CH:30]=[CH:31][C:24]([O:23][CH2:22][CH2:21][CH2:20][N:14]2[CH2:19][CH2:18][CH2:17][CH2:16][CH2:15]2)=[CH:25][CH:26]=1Participants
4
Procedure
The entitled compound was obtained according to the method of Example 15 but starting from 2-amino-4-methylbenzoic acid, methylamine and 4-(3-piperidin-1-ylpropoxy)benzaldehyde.
Workup
- customThe entitled compound was obtained
Sources & evidence
- ORD record
- ord-c359c20521fb4f208fdb7bd18224d4f5
- Source dataset
- uspto-grants-2011_06
- Patent number
- US07960394B2
Reaction notes
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