Methylamine → HCID 11574753, compound
Reaction equation
[NH2:1][C:2]1[C:10]([O:11][CH3:12])=[N:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=O.[CH3:13][NH2:14].[N:15]1([CH2:20][CH2:21][CH2:22][O:23][C:24]2[CH:31]=[CH:30][C:27]([CH:28]=O)=[CH:26][CH:25]=2)[CH2:19][CH2:18][CH2:17][CH2:16]1>>[CH3:12][O:11][C:10]1[C:2]2[N:1]=[C:28]([C:27]3[CH:30]=[CH:31][C:24]([O:23][CH2:22][CH2:21][CH2:20][N:15]4[CH2:19][CH2:18][CH2:17][CH2:16]4)=[CH:25][CH:26]=3)[N:14]([CH3:13])[C:4](=[O:6])[C:3]=2[CH:7]=[CH:8][N:9]=1Participants
4
Procedure
The entitled compound was obtained according to the method of Example 15 but starting from 3-amino-2-methoxyisonicotinic acid, methylamine and 4-(3-pyrrolidin-1-ylpropoxy)benzaldehyde.
Workup
- customThe entitled compound was obtained
Sources & evidence
- ORD record
- ord-587cf249da5542fbbd087c8af76f84c8
- Source dataset
- uspto-grants-2011_06
- Patent number
- US07960394B2
Reaction notes
Loading…