Methylamine → HCID 67244445, compound
Reaction equation
[NH2:1][C:2]1[CH:10]=[CH:9][C:8]([N+:11]([O-:13])=[O:12])=[CH:7][C:3]=1[C:4]([OH:6])=O.[CH3:14][NH2:15].[N:16]1([CH2:22][CH2:23][CH2:24][O:25][C:26]2[CH:27]=[C:28]([CH:31]=[CH:32][CH:33]=2)[CH:29]=O)[CH2:21][CH2:20][CH2:19][CH2:18][CH2:17]1>>[CH3:14][N:15]1[C:4](=[O:6])[C:3]2[C:2](=[CH:10][CH:9]=[C:8]([N+:11]([O-:13])=[O:12])[CH:7]=2)[N:1]=[C:29]1[C:28]1[CH:31]=[CH:32][CH:33]=[C:26]([O:25][CH2:24][CH2:23][CH2:22][N:16]2[CH2:21][CH2:20][CH2:19][CH2:18][CH2:17]2)[CH:27]=1Participants
4
Procedure
The intended compound was obtained according to the method of Example 15 but using 2-amino-5-nitrobenzoic acid, methylamine and 3-(3-piperidin-1-ylpropoxy)benzaldehyde.
Workup
- customThe intended compound was obtained
Sources & evidence
- ORD record
- ord-e4e467bc26a3495b926b5a8143cf9dce
- Source dataset
- uspto-grants-2011_06
- Patent number
- US07960394B2
Reaction notes
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