Methylamine → HCID 11641382, compound

HRID 2422647Notes

Reaction equation

HRID 2422647 reaction equation
[Br:1][C:2]1[CH:10]=[C:6]([C:7]([OH:9])=O)[C:5]([NH2:11])=[CH:4][CH:3]=1.[CH3:12][NH2:13].[OH:14][C:15]1[CH:22]=[CH:21][C:18]([CH:19]=O)=[C:17]([O:23][CH3:24])[CH:16]=1.[Br-].Br[CH2:27][CH2:28][CH2:29][NH+:30]1[CH2:34][CH2:33][CH2:32][CH2:31]1>>[Br:1][C:2]1[CH:10]=[C:6]2[C:5](=[CH:4][CH:3]=1)[N:11]=[C:19]([C:18]1[CH:21]=[CH:22][C:15]([O:14][CH2:27][CH2:28][CH2:29][N:30]3[CH2:34][CH2:33][CH2:32][CH2:31]3)=[CH:16][C:17]=1[O:23][CH3:24])[N:13]([CH3:12])[C:7]2=[O:9]

Participants

5

Reactant 4

HCID 6329MethylamineHCID 798582-Amino-5-bromobenzoic acidHCID 5195414-Hydroxy-2-MethoxybenzaldehydeHCID 178419552HCID 178419552, compound

Product 1

HCID 11641382HCID 11641382, compound

Procedure

The entitled compound was obtained according to the method of Example 77 but using 5-bromoanthranilic acid, methylamine, 4-hydroxy-2-methoxybenzaldehyde and 1-(3-bromopropyl)pyrrolidinium bromide.

Workup

  1. customThe entitled compound was obtained

Sources & evidence

ORD record
ord-8f1e0996020a4fda88d43250b56ca908
Source dataset
uspto-grants-2011_06
Patent number
US07960394B2

Reaction notes

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