Methylamine → HCID 11703898, compound

HRID 2422648Notes

Reaction equation

HRID 2422648 reaction equation
[NH2:1][C:2]1[N:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=O.[CH3:11][NH2:12].[CH3:13][O:14][C:15]1[CH:22]=[C:21]([OH:23])[CH:20]=[CH:19][C:16]=1[CH:17]=O.[Br-].Br[CH2:26][CH2:27][CH2:28][NH+:29]1[CH2:33][CH2:32][CH2:31][CH2:30]1>>[CH3:13][O:14][C:15]1[CH:22]=[C:21]([O:23][CH2:26][CH2:27][CH2:28][N:29]2[CH2:33][CH2:32][CH2:31][CH2:30]2)[CH:20]=[CH:19][C:16]=1[C:17]1[N:12]([CH3:11])[C:4](=[O:6])[C:3]2[CH:7]=[CH:8][CH:9]=[N:10][C:2]=2[N:1]=1

Participants

5

Reactant 4

HCID 6329MethylamineHCID 729302-Aminonicotinic acidHCID 5195414-Hydroxy-2-MethoxybenzaldehydeHCID 178419552HCID 178419552, compound

Product 1

HCID 11703898HCID 11703898, compound

Procedure

The entitled compound was obtained according to the method of Example 77 but using 2-aminonicotinic acid, methylamine, 2-methoxy-4-hydroxybenzaldehyde and 1-(3-bromopropyl)pyrrolidinium bromide.

Workup

  1. customThe entitled compound was obtained

Sources & evidence

ORD record
ord-b7a628ebfb4b45879261a342b1cf6c5a
Source dataset
uspto-grants-2011_06
Patent number
US07960394B2

Reaction notes

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