HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 11517340, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Cyclobutanone | HCID 14496 | — |
| Reactant | 4-Methoxybenzaldehyde | HCID 31244 | — |
| Reactant | 2-Amino-3-methoxybenzoic acid | HCID 255720 | — |
| Reactant | Tert-butyl 4-hydroxypiperidine-1-carboxylate | HCID 643502 | — |
| Product | HCID 11517340 | HCID 11517340 | — |
Reaction Steps
The entitled compound was obtained according to the method of Example 85 but using 2-amino-3-methoxybenzoic acid, methylamine, 4-methoxybenzaldehyde, tert-butyl 4-hydroxytetrahydro-1(2H)-pyridinecarboxylate, and cyclobutanone. The obtained compound was recrystallized from ethyl acetate-heptane to give a colorless acicular crystal (m.p. 201.0-204.0° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07960394B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-015e8eb4a64041e9b9c278b28fe6d150 |
| Source note | uspto-grants-2011_06 |