HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 86628705, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 86628704 | HCID 86628704 | — |
| Product | HCID 86628705 | HCID 86628705 | — |
Reaction Steps
A mixture of acid 17 (200 mg, 0.685 mmol) and thionyl chloride (1 ml) was heated at reflux for 1.5 h. The excess thionyl chloride was removed in vacuo and the residue dried under high vacuum at 50° C. for 1.5 h. The product acid chloride 18 was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07960434B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-8a4a5640e8f64b03b2048aae9e605d92 |
| Source note | uspto-grants-2011_06 |