HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloroaniline → N-(Benzimidazol-2-yl)-4-chloroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloroaniline | HCID 7812 | — |
| Reactant | 2-Chlorobenzimidazole | HCID 78572 | — |
| Product | N-(Benzimidazol-2-yl)-4-chloroaniline | HCID 923854 | — |
Reaction Steps
The title compound was prepared from 2-chlorobenzimidazole and 4-chloroaniline by Procedure A. The product was isolated by filtration and recrystallisation to give the title compound as a hydrochloride salt (white solid, mp 238-240° C.). MS(ES+) m/z 244 ([M+1]+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07960561B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-2d1e7315dc5a47db839f4fc3cba28783 |
| Source note | uspto-grants-2011_06 |