HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminobenzonitrile → 3-[(1H-Benzimidazol-2-yl)amino]benzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminobenzonitrile | HCID 16702 | — |
| Reactant | 2-Chlorobenzimidazole | HCID 78572 | — |
| Product | 3-[(1H-Benzimidazol-2-yl)amino]benzonitrile | HCID 15602786 | — |
Reaction Steps
The title compound was prepared from 2-chlorobenzimidazole and 3-aminobenzonitrile by Procedure A. The product was isolated by filtration and preparative LCMS to give the title compound as the free base (white solid, mp 272-274° C.). MS(ES+) m/z 235 ([M+1]+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07960561B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-25b64aee81f440588a0155b02c69c9b5 |
| Source note | uspto-grants-2011_06 |